2002标定数据

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1、常减压蒸馏装置标 定 数 据 汇 总 表标定日期：2002年9月18日南充炼油化工总厂一车间2002 年 10 月 5 日原油：川中原油表-1物料平衡序号物料名称流量 t/h产量 t/d收率 %1原油63.821531.682初顶汽油7.42178.0811.633常顶汽油4.64111.367.274溶剂油1.5837.922.485煤油1.3833.122.166柴油15.63375.1224.497常四线1.6840.322.638减顶油0.061.440.099减一线3.6086.405.6410减二线4.20100.86.5811减三线5.9141.69.2412减四线1.945.6

2、2.9813减渣15.21365.0423.8314不凝气0.37.20.4715损失0.327.680.516轻质油拔出率48.0317常压拔出率50.6618减压拔出率24.5419总拔出率75.2015表-2 馏出口质量分析结果样品名称比重D420馏 程，残炭%运动粘度恩氏粘度闪点比色酸度酸值凝点HK2%10%30%50%70%90%97%KK馏出20508010050100初顶油717.744.872.993107.6119.6145161.6960.52拔头油852.81882192663464194891.2617.485.0190.0224常顶油738.478.396106.81

3、16.6127.4140.2161.2970.569常一线766.8150.8153.6157.6159.6162.5166.5185.2189.298.50.777390常二线772.3175.7177.7178.7181.7184.5190.5200.4980.97854.9常三线804.4182.1209.5233.2253.2279.4309.5326.5981.9911.30658.4-8常四线828.92903463663723793873923966.6382.5551.49167常一中766.1148.7153.9159.9164167171184.3991.130.794常二

4、中820.5235.6271.2303316327336345993.9252.295样品名称比重D420馏 程，残炭%运动粘度恩氏粘度闪点比色酸度酸值凝点HK2%10%30%50%70%90%97%KK馏出20508010050100常渣油872.12633213844334745001.910.1683减顶油810.9124.3150.7181.2220257.2300.8331.8991.4181.013减一线831.82583223353513643683833941.4713.4921.4616850.0168减二线845.53483823903964004074315.8784.0

5、392.021.3120890.0084减三线858.93754134264394494584744799.2966.0141.5235130.0084减四线867.233942145648550415.819.6431.94257180.014减一中835.928033735336937938740114.315.9742.240.1402减二中852.92793924004134204284424506.6224.4052.271.350.1318减渣油8973184505135294.090.1402表-3原 油 性 质 分 析样品名称重金属分析ppm密度kg/m3水分%含盐mg/l含沙

6、%凝点酸值mg/g残炭%运动粘度馏程，350%50100HK10%20%30%40%50%70%脱前原油铁8.89镍0.87钒0.94(脱前)840.548740.13526.20.0811.027.587125.7165.4236.1293.835050一级脱后原油830.4痕迹8二级脱后原油830.7痕迹7三级脱后原油841.6无3表-4气 体 分 析分析项目名称H2O2N2COCO2H2SNONO2NOXCH4C2C3异丁烷正丁烷丁烯C5天然气 %21.3000075.62.80.30.1000初不凝气 %1.1000038.311.324.25.812.606.7常不凝气 %00000

7、000099.780.020.060.050.010.030.05减不凝气 %17.60000000049.316.270.44.03.42.1炉-1烟气体积浓度ppm11.405.5078078质量浓度mg/ m3001040160炉-2烟气体积浓度ppm6.8608.1311040104质量浓度mg /m3011390213表-5水质分析项目容91容92PH值1212硫化物60.74mg/L72.67mg/LCL2.66mg/L3.99mg/L测定日温度：28.5大气压：98.210hPa风速：1.4m/s表6 初 馏 塔 标 定 数 据 初馏塔温度，塔顶压力MPa塔底液面，%容-2液面，

8、%容-2界面，%闪蒸段压力(现场)MPa塔顶压力(现场)MPa塔顶冷回流量T/H容2压力MPa初馏塔表面温度进料塔顶闪蒸段塔底回流190125186189510.123365510.1180.11120.970.0955表7 常 压 塔 标 定 数 据 操作温度，进料塔顶回流温度闪蒸段塔底一线抽出二线抽出三线抽出四线抽出一中抽出一中返回二中抽出二中返回36层汽相26层汽相18层汽相10层汽相3601214434534715819024832017480307147182189277327压力，MPa液位，%流量，T/H塔表温度塔顶塔顶(现)闪蒸段(现)容3容3液位容3界位一线二线三线四线塔底冷

9、回流一中回流二中回流过热蒸汽0.0860.070.11654576403050427.8221.48.41.1863表8 减 压 塔 标 定 数 据 操作温度，进料塔顶回流温度闪蒸段塔底一线抽出二线抽出三线抽出四线抽出一中抽出一中返回二中抽出二中返回一段填料上汽21层汽相二段填料下汽三段填料下洗涤油入塔塔表温度转油线末端3881016337319726132235224414629015020228835836431741真空度，KPa抽空蒸汽压力液位，%流量，T/H塔顶塔顶(现)闪蒸段(现)转油线末端一段填料上二线返回上三线返回上四线抽出一线二线三线四线塔底 一线回流一中回流二中回流过热蒸汽

10、抽空蒸汽93.6949290697510575404.9918.660.04表9 抽 空 系 统 标 定 数 据真空度,kPa温度,压力,MPa抽-1前抽-1后抽-2前冷-9油气冷-9水冷-10油气冷-10水冷-11油气冷-11水循环水循环水抽空蒸汽95949323.227.547.14152.129.826.70.310.83表10 加 热 炉 标 定 数 据常压炉温度,常压炉压力,MPa换热终温对流出口辐射出口过热蒸汽炉膛烟气出对流室烟气入预热器烟气出预热器热风炉膛负压进炉出炉燃料气热风烟气出预热器264296360397636370331209191250Pa0.90.150.40.00

11、4减压炉温度,减压炉压力,MPa常压炉表面温度进口对流出口辐射出口炉膛1炉膛2烟气炉表面炉膛负压进炉出炉38965163439977.5150Pa0.260.00972.2表11 换热器标定数据编 号介 质温 度压 力MPa型号进口出口进口出口换-1/1.2管程减一线19068.90.80BES500-4-55-6/25-4I壳程原油45601.601.55换-2管程常四线195700.990.98BES500-2.5-55-6/25-4壳程原油6062.41.551.50换-3/1.2管程常一中161860.490.47BES600-2.5-85-6/25-4壳程原油62.4901.501.

12、36换-4/1.2管程原油901021.361.33BES600-4-90-6/25-2I壳程减渣150920.18换-5管程原油102109.31.331.30BES600-2.5-85-6/25-4I壳程减二线207115.70.930.90换-6管程原油109.31151.301.27BES600-4-85-6/25-4I壳程减三线2101300.81换-7管程常二线1401220.87BES500-2.5-55-6/25-4壳程原油115116.71.271.25换-8/1.2管程常三线1541351.02BES500-2.5-55-6/25-4壳程原油116.71271.251.16

13、换-9管程原油1271341.121.10BES500-2.5-55-6/25-2I壳程减四线3501240.8换-10管程减一中1801640.49BES600-2.5-85-6/25-4I壳程原油1341421.101.03换-11管程原油1421461.030.98BES600-2.5-90-6/25-2I壳程减渣1821500.290.18换-12管程常一中181.81530.48BES600-2.5-85-6/25-4I壳程脱盐油1281390.980.93换-13管程脱盐油1311430.930.87BES500-2.5-55-6/25-2I壳程常三线1901541.061.02换

14、-14/1.2管程常二中2051620.58BES500-2.5-55-6/25-4壳程脱盐油143153.30.870.76换-15/1.2管程减二中192164.50.53BES600-2.5-85-6/25-4壳程脱盐油153.31580.760.66续表-11换热器标定数据编 号介 质温 度压 力MPa型号进口出口进口出口换-16管程减一中2401800.530.49BES500-2.5-55-6/25-4壳程脱盐油1581650.660.56换-17管程脱盐油1651720.560.51BES600-2.5-90-6/25-2I壳程减渣1891820.320.29换-18/1.2管程

15、脱盐油1721850.510.4BES500-2.5-55-6/25-4壳程常三线2451901.11.06换-19/1.2管程脱盐油1851900.400.20BES600-4-90-6/25-2I壳程减渣2761890.360.32换-20管程减二中2231920.60.53BES500-2.5-55-6/25-4壳程初底油1891941.81.75换-21管程初底油1941971.751.70BES600-4-85-6/25-4I壳程常四线2551951.050.99换-22管程初底油1972001.71.64BES600-4-90-6/25-4I壳程减二线2502070.950.93换

16、-23/1.2管程常二中2542050.710.58BES600-4-85-6/25-4I壳程初底油2002051.641.58换-24/1.2管程初底油2052101.581.50BES500-2.5-55-6/25-2I壳程减三线3002100.90.81换-25/1.2管程减二中2902230.620.6BES600-4-85-6/25-4I壳程初底油2102161.501.4换-26/1.2管程初底油2162351.41.3BES600-4-90-6/25-2I壳程减渣3152760.440.36换-27管程常四线3102551.11.05BES500-4-55-6/25-4I壳程初底

17、油2352401.31.25换-28/1.2管程初底油2403301.251.16BES600-4-90-6/25-2I壳程常二中3072540.80.71换-29/1.2管程初底油2502641.161.06BES600-4-90-6/25-2I壳程减渣3733150.70.44换-30/1.2管程脱盐水1280.55AES400-4-30-6/25-4壳程新鲜水45901.21.2BES400-4-30-6/25-2I注：换热器温度用测温仪测定，误差较大。表-12冷却器标定数据编 号介 质温 度型号进口出口冷-1/1-4空冷初顶油12574X4.52-4-39-16S-23.4/RL-Ia

18、冷-2管程循环水2832BES800-1.6-160-6/25-4II壳程初顶油7860冷-3/1-4空冷常顶油12189X4.53-4-61-16S-23.4/RL-Ia 冷-4/1.2管程循环水2559FA600-105-25-4壳程常顶油8949FB500-25-55-6/25-4冷-5管程循环水2833BES600-1.6-85-6/25-4壳程常一线10928冷-6管程循环水2833BES500-2.5-55-6/25-4壳程常二线12033.7冷-7管程循环水2845.6BES500-2.5-90-6/25-4壳程常三线12044.5冷-8管程循环水2848.7BES500-2.5

19、-55-6/25-4壳程常四线6965.7冷-9管程循环水BJS800-1.6-160-6/25-4壳程减顶油冷-10管程循环水BJS800-1.6-160-6/25-4壳程减顶油冷-11管程循环水FLB700-125-16-2壳程减顶油冷-12管程循环水2827.6BES500-2.5-55-6/25-4壳程减一线6962冷-13管程循环水2870BES500-2.5-55-6/25-4壳程减二线111109.6冷-14管程循环水28113BES500-2.5-55-6/25-4壳程减三线13090冷-15管程循环水2832BES400-4-30-6/25-4壳程减四线12092冷-16/1

20、.2管程循环水2853BES500-2.5-55-6/25-2I壳程减渣9284表13 机泵标定数据编号设备名称型号出口压力，MPa 实测电流，A1/1.2原油泵100AY1202A1.91342/1.2初底油泵100AY1202A1.81133/1.2常底油泵80AY1002A1.34/1.2减底油泵65AY1002B1.055/1.2初顶油泵65AY600.76/1.2常顶油泵65AY600.510.27常一线油泵40AY402B8/1.2常二线油泵50AY602B0.959/1.2常三线油泵65AY1002C1.110常四线油泵50AY6021.011/1.2常一中泵80AY601.15

21、12常二中泵65AY600.6514/1.2减一线泵65AY100A0.820.915/1.2减二线泵50AY602A0.91316/1.2减三线泵50AY602A0.913.217减四线泵50AY602A0.818.918/1.2减一中泵65AY600.619减二中泵65AY600.621/1注水泵DY125031.5521/2注水泵DY62571.621/3-5循环注水泵50AY601.722/1.2原油注碱泵1DB0.06/1.523/1-3破乳剂泵J-Z200/1.624/1缓蚀剂泵J-Z200/1.624/2缓蚀剂泵1DB-0.06/1.524/3缓蚀剂泵J-D800/3.225/1汽油碱洗泵32W-3025/2汽油碱洗泵32W-7525/3煤油碱洗泵32W-7525/4柴油水洗泵40W-9025/5柴油碱洗泵40W-9029/1初顶碱洗泵32W-7529/2.3常顶碱洗泵32W-7531/1.2氨水泵JX-50/1.0